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STRUCTURE AND MAGNETIC PROPERTIES OF STRONTIUM HEXAFERRITE POWDER AFTER MILLING IN WATER AND TOLUENE AND FOLLOWING ANNEALING

https://doi.org/10.17073/1609-3577-2013-2-65-68

Abstract

Structural changes of strontium hexaferrite powders after milling in water and toluene and after subsequent annealing were studied using X-ray diffraction, Scanning Electron Microscopy and Laser diffraction. Also magnetic properties changes were studied. The coarse-grain powder milling leads to an abrupt decrease of its particles size and the average crystallite size as well as an increase of SrFe12O19 phase lattice microstrains. Saturation magnetization and remanence decrease after milling in both media. At the same time coercive force of milled powders changes insignificantly with increasing milling time. The subsequent annealing allowed us to increase the magnetic properties of the powder. The annealed powders are characterized by the following magnetic properties: µ0Нci = 0,42¸0,49 T, µ 0Ir = 0,23¸0,24 T, (BH)max = 8-9,6 kJ/m3.

About the Authors

T. A. Bulatov
National University of Science and Technology MISiS
Russian Federation


S. V. Ketov
National University of Science and Technology MISiS
Russian Federation


V. P. Menushenkov
National University of Science and Technology MISiS
Russian Federation


Yu. D. Yagodkin
National University of Science and Technology MISiS
Russian Federation


References

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For citations:


Bulatov T.A., Ketov S.V., Menushenkov V.P., Yagodkin Yu.D. STRUCTURE AND MAGNETIC PROPERTIES OF STRONTIUM HEXAFERRITE POWDER AFTER MILLING IN WATER AND TOLUENE AND FOLLOWING ANNEALING. Izvestiya Vysshikh Uchebnykh Zavedenii. Materialy Elektronnoi Tekhniki = Materials of Electronics Engineering. 2013;(2):65-68. (In Russ.) https://doi.org/10.17073/1609-3577-2013-2-65-68

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ISSN 1609-3577 (Print)
ISSN 2413-6387 (Online)